Peer-reviewedCC BYActa crystallographica. Section E, Crystallographic communications
Synthesis and structure of 1,1-bis-(furan-2-ylmethyl)-3-phenyl-urea.
6 affiliations
- 1RUDN University, 6 Miklukho-Maklaya St., Moscow 117198, Russian Federation.
- 2Zelinsky Institute of Organic Chemistry of RAS, Leninsky Prospect 47, Moscow 119991, Russian Federation.
- 3Hacettepe University, Department of Physics, 06800 Beytepe-Ankara, Türkiye.
- 4Department of Chemistry, Bahir Dar University, PO Box 79, Bahir Dar, Ethiopia.
- 5Azerbaijan Medical University, Scientific Research Centre (SRC), A. Kasumzade Str. 14, AZ 1022, Baku, Azerbaijan.
- 6Department of Chemical Engineering, Baku Engineering University, Hasan Aliyev Str. 120, AZ0101, Khirdalan, Absheron, Azerbaijan.
Abstract
The asymmetric unit of the title compound, C17H16N2O3, contains two mol-ecules, A and B, with one furan ring in each mol-ecule showing 'flip' rotational disorder. In the crystal, N-H⋯O hydrogen bonds link the mol-ecules into separate infinite ⋯A⋯A⋯A⋯ and ⋯B⋯B⋯B⋯ chains propagating along the c-axis direction. Weak C-H⋯π inter-actions may help to consolidate the packing. Hirshfeld surface analysis revealed that the most important contributions to the packing are from H⋯H, H⋯C/C⋯H and H⋯O/O⋯H inter-actions with very similar surface percentages for both mol-ecules.
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BibTeX
@article{mertsalov2026synthesis,
title = {{Synthesis and structure of 1,1-bis-(furan-2-ylmethyl)-3-phenyl-urea.}},
author = {Dimitriy F Mertsalov and Dimitriy M Schevnikov and Victor N Khrustalev and Tuncer Hökelek and Alebel N Belay and Khudayar I Hasanov and Ibadulla H Mahmudov},
journal = {Acta crystallographica. Section E, Crystallographic communications},
year = {2026},
month = oct,
doi = {10.1107/s2056989026010029},
url = {https://europepmc.org/article/MED/42997285},
note = {CC BY},
}
RIS
TY - JOUR
TI - Synthesis and structure of 1,1-bis-(furan-2-ylmethyl)-3-phenyl-urea.
AU - Dimitriy F Mertsalov
AU - Dimitriy M Schevnikov
AU - Victor N Khrustalev
AU - Tuncer Hökelek
AU - Alebel N Belay
AU - Khudayar I Hasanov
AU - Ibadulla H Mahmudov
PY - 2026
DA - 2026/10/02
JO - Acta crystallographica. Section E, Crystallographic communications
DO - 10.1107/s2056989026010029
UR - https://europepmc.org/article/MED/42997285
AB - The asymmetric unit of the title compound, C17H16N2O3, contains two mol-ecules, A and B, with one furan ring in each mol-ecule showing 'flip' rotational disorder. In the crystal, N-H⋯O hydrogen bonds link the mol-ecules into separate infinite ⋯A⋯A⋯A⋯ and ⋯B⋯B⋯B⋯ chains propagating along the c-axis direction. Weak C-H⋯π inter-actions may help to consolidate the packing. Hirshfeld surface analysis revealed that the most important contributions to the packing are from H⋯H, H⋯C/C⋯H and H⋯O/O⋯H inter-actions with very similar surface percentages for both mol-ecules.
SN - 2056-9890
ER -