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Peer-reviewedCC BYScience and technology of advanced materials

Dendrite-scale quantitative evaluation of solidification cracking in welding using in-situ synchrotron X-ray imaging: distribution characteristics of critical strain.

  1. 1Research Center for Structural Materials, National Institute for Materials Science, Tsukuba, Ibaraki, Japan.
  2. 2Joining and Welding Research Institute, The University of Osaka, Ibaraki, Osaka, Japan.

Abstract

Solidification cracking is a critical defect in welding, and its occurrence has conventionally been described using temperature-dependent critical-strain curves. However, whether the critical strain is uniquely determined by temperature remains unclear, particularly at the dendrite scale. In this study, solidification-cracking behavior in an Fe-15Mn-10Cr-8Ni-4Si alloy was investigated using in-situ synchrotron X-ray transmission imaging combined with local strain and temperature analyses. Crack-initiation events were identified from the time-resolved X-ray images, and the corresponding critical equivalent strains and critical temperatures were extracted at individual positions along the crack path. Solidification cracking occurred over approximately 1320-1000°C, corresponding to the effective solid-liquid coexistence region predicted by a Scheil-Gulliver calculation. The median critical strain was higher at lower temperatures and generally decreased toward higher temperatures. A broad critical-strain distribution remained within each 30°C temperature range. After subtraction of the temperature-bin median, the remaining variation was spatially nonuniform along the crack path. Comparison with a non-cracking case showed that most equivalent-strain values remained below the critical-strain distribution obtained in the cracking case, although the upper tail partially overlapped its lower part. These results provide experimental evidence that the critical strain at solidification-crack initiation is better represented as a temperature-dependent distribution than as a single-valued curve. The physical factors governing the distribution width and spatial variation remain to be identified.

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BibTeX
@article{kitano2026dendritescale,
  title = {{Dendrite-scale quantitative evaluation of solidification cracking in welding using in-situ synchrotron X-ray imaging: distribution characteristics of critical strain.}},
  author = {Houichi Kitano and Tomoya Nagira and Fumiyoshi Yoshinaka and Takahiro Sawaguchi and Takayuki Yamashita and Yasuhiro Aoki and Hidetoshi Fujii},
  journal = {Science and technology of advanced materials},
  year = {2026},
  month = oct,
  doi = {10.1080/14686996.2026.2736326},
  url = {https://europepmc.org/article/MED/42910337},
  note = {CC BY},
}
RIS
TY  - JOUR
TI  - Dendrite-scale quantitative evaluation of solidification cracking in welding using in-situ synchrotron X-ray imaging: distribution characteristics of critical strain.
AU  - Houichi Kitano
AU  - Tomoya Nagira
AU  - Fumiyoshi Yoshinaka
AU  - Takahiro Sawaguchi
AU  - Takayuki Yamashita
AU  - Yasuhiro Aoki
AU  - Hidetoshi Fujii
PY  - 2026
DA  - 2026/10/12
JO  - Science and technology of advanced materials
DO  - 10.1080/14686996.2026.2736326
UR  - https://europepmc.org/article/MED/42910337
AB  - Solidification cracking is a critical defect in welding, and its occurrence has conventionally been described using temperature-dependent critical-strain curves. However, whether the critical strain is uniquely determined by temperature remains unclear, particularly at the dendrite scale. In this study, solidification-cracking behavior in an Fe-15Mn-10Cr-8Ni-4Si alloy was investigated using in-situ synchrotron X-ray transmission imaging combined with local strain and temperature analyses. Crack-initiation events were identified from the time-resolved X-ray images, and the corresponding critical equivalent strains and critical temperatures were extracted at individual positions along the crack path. Solidification cracking occurred over approximately 1320-1000°C, corresponding to the effective solid-liquid coexistence region predicted by a Scheil-Gulliver calculation. The median critical strain was higher at lower temperatures and generally decreased toward higher temperatures. A broad critical-strain distribution remained within each 30°C temperature range. After subtraction of the temperature-bin median, the remaining variation was spatially nonuniform along the crack path. Comparison with a non-cracking case showed that most equivalent-strain values remained below the critical-strain distribution obtained in the cracking case, although the upper tail partially overlapped its lower part. These results provide experimental evidence that the critical strain at solidification-crack initiation is better represented as a temperature-dependent distribution than as a single-valued curve. The physical factors governing the distribution width and spatial variation remain to be identified.
SN  - 1468-6996
SN  - 1878-5514
ER  -