Peer-reviewedCC BYJournal of Spectroscopy
Electrospray Tandem Mass Spectrometry of Ecdysteroid Moulting Hormones
Abstract
Electrospray mass spectrometIy has aided the structural characterization of ecdysteroid moulting hormones as a means of understanding factors controlling the moulting cycle in crabs. Possible fragmentation routes were frrst obtained by controlled collision‐activated dissociation (CAD) initiated by cone voltage fragmentation. Low energy CAD MSIMS analyses of the protonated molecules [M+H]+ confrrmed the characteristic fmgerprint patterns obtained by cone voltage fragmentation. MSIMS analyses of selected intermediate fragments provided additional structural data and established the fragmentation routes.
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BibTeX
@article{hellou2026electrospray,
title = {{Electrospray Tandem Mass Spectrometry of Ecdysteroid Moulting Hormones}},
author = {Jocelyne Hellou and Joseph Banoub and Emmanuel Gentil and Dave Taylor and Paul O’keefe},
journal = {Journal of Spectroscopy},
year = {2026},
month = sep,
doi = {10.1155/1994/982952},
url = {https://hal.science/hal-05742275v1},
note = {CC BY},
}
RIS
TY - JOUR
TI - Electrospray Tandem Mass Spectrometry of Ecdysteroid Moulting Hormones
AU - Jocelyne Hellou
AU - Joseph Banoub
AU - Emmanuel Gentil
AU - Dave Taylor
AU - Paul O’keefe
PY - 2026
DA - 2026/09/08
JO - Journal of Spectroscopy
DO - 10.1155/1994/982952
UR - https://hal.science/hal-05742275v1
AB - Electrospray mass spectrometIy has aided the structural characterization of ecdysteroid moulting hormones as a means of understanding factors controlling the moulting cycle in crabs. Possible fragmentation routes were frrst obtained by controlled collision‐activated dissociation (CAD) initiated by cone voltage fragmentation. Low energy CAD MSIMS analyses of the protonated molecules [M+H]+ confrrmed the characteristic fmgerprint patterns obtained by cone voltage fragmentation. MSIMS analyses of selected intermediate fragments provided additional structural data and established the fragmentation routes.
SN - 2314-4920
SN - 2314-4939
ER -